ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India – Download as PDF File .pdf), Text File .txt) or read online. ASTM A Practice A test (Oxalic acid test). The oxalic acid etch test is rapid and nondestructive, but not quantitative. It is a rapid etching procedure and . Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.

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In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away.

The Oxalic Acid test is also only applicable x corrosion associated with chromium carbide precipitates and is only useful for specific material grades. Contact us now for pricing or a quote!

The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. Discover perspectives, resources, and advice from our world-leading Engaged Experts.

Wilson Hardness Conversion Chart.

Intergranular Corrosion Testing: An Overview of ASTM A262

A different ASTM A test method must be used to quantify the level of corrosion or to disqualify a material for use. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date. Like what you saw? ASTM A is a common intergranular corrosion testing method that can quickly screen batches of material to determine corrosion susceptibility. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.

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Intergranular Attack – ASTM A – Colorado-Metallurgical-Services

It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.

ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. In everyday pracrice, corrosion varies by materials and solutions.


All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. Plating and Coating Testing.

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This method is preferable for chromium depletions and corrosion in intermetallic phases. Classification of structure then provides either acceptance or further testing required, which typically moves you to one of the next practices.

The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results.

Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. Link to Active This link will always route to the current Active version of the standard. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared.

Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

This specification is for detecting susceptibility to intergranular attack IGA. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.

The inch-pound equivalents are in parentheses and may be approximate. asstm

ASTM A Testing: An Overview of Intergranular Corrosion | Element

Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.

If you are not sure, please contact us for assistance. Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

G2MT Labs is one of the few labs to offer all asm ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and ast corrosion consulting as needed.

It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


Because it can be run quickly for screening, we often run this test first. The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”. This abstract is a brief summary of the referenced standard. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion.

Practice B, also known lractice the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance.

These practices include five intergranular corrosion tests, namely: Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. If the structure is acceptable no additional testing is required. The ASTM A practie can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use.

Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. Due to the variance of attack in different materials, numerous methods Prcatice B-F are used to assess intergranular corrosion.

The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. wstm

A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.

It depends on which Practice is selected, but typically ranges from to practiec for lractice tests. The level of corrosion is determined by mass loss. The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. Carbon and Sulfur Analysis.

Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack.